Table 3. GC-MS parameters

Oven temperature program: Rate (°C/min) Temp (°C) Hold time (min)
50 0
15 120 0
10 300 15
Injection volume: 1.0 μL; Injection mode: Splitless; Carrier gas flow rate: 1 mL/min.
MS parameters: MS ionization mode: Electron ionization (70 eV); Acquisition mode: Scan; Mass range: 50 to 550 amu.
GC-MS: gas chromatography-mass spectrometry.