Table 3. Water-insoluble solid residue (WIS) and residual ratio of each component pretreated with Liriodendron tulipifera depending on the temperature (based on each initial content in unpretreated L. tulipifera)
Temp. (°C) | WIS (%) | Structural sugars (%) | Lignins (%) | Total (g) |
Glucan | Xylan | Total | Klason lignin | Acid soluble lignin | Total |
Unpret. | 100.0 | 100.0 | 100.0 | 100.0 | 100.0 | 100.0 | 100.0 | 100.0 |
120 | 92.1 ± 0.1 | 100.0 ± 0.2 | 100.0 ± 1.0 | 100.0 ± 0.7 | 87.1 ± 0.4 | 89.8 ± 0.4 | 87.4 ± 0.3 | 97.8 ± 0.5 |
130 | 83.1 ± 1.0 | 96.6 ± 0.7 | 78.7 ± 0.2 | 90.7 ± 1.2 | 77.0 ± 0.6 | 78.8 ± 0.2 | 77.2 ± 0.2 | 86.8 ± 0.6 |
140 | 75.6 ± 1.5 | 97.3 ± 0.3 | 58.1 ± 0.5 | 84.4 ± 0.6 | 69.1 ± 0.3 | 64.4 ± 0.6 | 68.4 ± 0.5 | 79.8 ± 0.6 |
150 | 60.0 ± 1.2 | 94.9 ± 0.5 | 28.3 ± 0.1 | 72.9 ± 0.5 | 43.8 ± 0.4 | 33.0 ± 0.3 | 42.3 ± 0.1 | 64.1 ± 0.3 |
160 | 51.9 ± 1.9 | 94.0 ± 0.5 | 16.6 ± 0.3 | 68.5 ± 0.2 | 31.4 ± 0.1 | 17.2 ± 0.2 | 29.4 ± 0.4 | 57.2 ± 0.3 |
170 | 44.1 ± 1.6 | 90.2 ± 0.7 | 5.0 ± 0.2 | 62.1 ± 0.4 | 20.4 ± 0.2 | 10.8 ± 0.4 | 19.0 ± 0.2 | 49.7 ± 0.3 |
180 | 40.0 ± 0.6 | 84.1 ± 0.4 | 0.0 ± 0.0 | 56.4 ± 0.3 | 19.1 ± 0.5 | 11.4 ± 0.1 | 18.0 ± 0.5 | 45.3 ± 0.4 |